Authors: | Frede, Timothy Aljoscha Burke, Inga Kockmann, Norbert |
Title: | Software-guided microfluidic reaction calorimeter based on thermoelectric modules |
Language (ISO): | en |
Abstract: | A software-guided, continuous reaction calorimeter based on thermoelectric modules for direct heat flux measurements is presented. Sensors and actuators of the calorimeter's setup are implemented within a lab automation system, which enables the automated calibration of the heat flux sensors and investigations of chemical reactions through sequential function charts. Functionality of the calibration is shown by heat transfer experiments. Additionally, the calorimeter's performance is demonstrated by good agreement of conducted neutralization experiments with literature data. |
Subject Headings: | Automated operation Continuous reaction calorimetry Heat flow calorimeter Isoperibolic reaction calorimetry Microcalorimeter |
URI: | http://hdl.handle.net/2003/40870 http://dx.doi.org/10.17877/DE290R-22727 |
Issue Date: | 2021-03-10 |
Rights link: | https://creativecommons.org/licenses/by/4.0/ |
Appears in Collections: | Arbeitsgruppe Apparatedesign |
Files in This Item:
File | Description | Size | Format | |
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Chemie Ingenieur Technik - 2021 - Frede - Software‐guided Microfluidic Reaction Calorimeter Based on Thermoelectric Modules.pdf | DNB | 1.61 MB | Adobe PDF | View/Open |
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